Farklı yapıdaki kompozit rezin materyallerinin su emilimi ve suda çözünürlük değerlerinin karşılaştırılması
Öz
Purpose: The aim of the study is to investigate the physical speciality of composite resins with the water sorption and solubility test.
Material and Method: With this aim, 6 kinds of composites were used like microhybrid (Venus), microfill hybrid (Gradia Direct Anterior), nanofill (Filtek Supreme) and nanohybrid composite resins (Clearfil Majesty Esthetic, Premise, Artemis). 15 samples were prepeared from each group at the standart dimensions. In the water sorption test, samples’ dried weight determined as M1. Samples were waited in pure water at 37 °C for 168 days and weight of samples were estimate with sensitive balance for 7 days period and determined as M2. M2 –M1/V formula were used to get results. In water solubility test samples’ dried weight determined as M1. Samples were waited in pure water at 37 °C for 168 days and weight of samples were estimate with sensitive balance for 7 days period and determined as M3. M3 –M1/V formula were used to get results. Data were analysed with statistically.
Results: In this in vitro study; in all tests, nanofill and nanohybrid composites according to micro hybrid and microfill hybrid composites was seen statistical meaningful.
Conclusion: At the result, composite resins including metacrylat group or groups, inorganic filling content, filler weight, resin matrix junctional surface affect the physical form.
ÖZET
Amaç: Kompozit rezinlerin fiziksel özelliklerinin; su absorbsiyonu ve çözünürlük testleri ile araştırılması amaçlanmıştır.
Gereç ve yöntem: Bu amaçla klinikte kullanılmakta olan universal(Venus), mikrofil hibrit (Gradia Direct Anterior), nanofil (Filtek Supreme) ve nanohibrit kompozit rezinler (Clearfil Majesty Esthetic, Premise, Artemis) olmak üzere 6 çeşit kompozit kullanılmıştır. Her bir gruptan standart boyutlarda 15 adet örnek hazırlanmıştır. Su absorbsiyon testinde örneklerin kuru ağırlıkları M1 olarak belirlendi. Örnekler 168 gün boyunca 37°C’ de distile suda bekletildi ve 7’şer günlük periyotlarla ağırlıkları hassas terazide ölçüldü ve M2 olarak belirlendikten sonra M2–M1/V formülüne göre sonuçlar mg/mm3 olarak tespit edildi. Çözünürlük testinde örneklerin kuru ağırlıkları M1 olarak belirlendi. Örnekler 168 gün boyunca 37°C’ de distile suda bekletildi ve 7’şer günlük periyotlarla ağırlıkları hassas terazide ölçüldü ve M3 olarak belirlendikten sonra M3–M1/V formülüne göre sonuçlar mg/mm3 olarak tespit edildi. Elde edilen verilerin istatistiksel de4erlendirilmesi yapıldı.
Bulgular: Yaptığımız in vitro çalışmadan elde ettiğimiz sonuçlara göre nanofil ve nano hibrit kompozitlerin tüm testlerde universal ve mikrofil hibrit kompozitlere göre istatistiksel olarak anlamlı fark oluşturduğu görülmüştür.
Sonuç: Sonuç olarak; kompozit rezinlerin içerdiği metakrilat grup veya grupların, inorganik doldurucu içeriğinin, doldurucu ağırlığının, rezin matriks bağlantı yüzeyinin fiziksel yapıyı etkilediği söylenebilir.
Anahtar kelimeler: Kompozit, su emilimi, suda çözünürlük
Anahtar Kelimeler
Kaynakça
- Craig RG. Direct esthetic restorative materials. Restorative Dental Materials 2000; 244-267.
- Hickel R, Dasch W, Janda R. New direct restorative materials. Int Dent J 1998; 48: 3-16.
- Manhart J, Kunzelmann KH, Chen HY, Hickel R. Mechanical properties and wear behavior of ligth-cure packable composite resins. Dent Mater 2000; 16:33-40.
- Dayangaç GB. Kompozit rezin restorasyonlar. Güne Kitapevi, Ankara, 2000, syf. 14.
- Guggenberger R, Weinmann W. Exploring beyond methacrylates. Am J Dent 2000; 30: 10-15.
- Mitra SB, Wu D, Holmes BM. An application of nanotechnology in advanced dental materials. J Am Dent Assoc ; 134: 1382-90.
- Condon JR, Ferracane JL. Reduced polymerization stres through non-bonded nanofillerparticles. Biomaterials 2002; 23: 3807- 3815.
- Dabano lu A, Kunzelmann KH, Hickel R, Koray F. Three- body wear resistance of resin composites.DGZ/EFCD-Meeting, Munich, Duke ES. Has dentistry moved into the nanotechnology era? Compend Contin Educ Dent 2003; 24: 380-82.
- Yap AU, Yap SH, Teo CK, Ng JJ. Comparison of surface finish of new aesthetic restorative materials. Oper Dent 2004; 29: 100-4.
- Bayne SC, Heymann HO, Swift EJ Jr. Update on dental composite restorations. J Am Dent Assoc 1994; 125: 687-701.
- Roberson TM, Heymann HO, Ritter AV. Introduction to composite restorations. Art&Science of operative dentistry, Ed. 4. St. Louis, Mosby Co Inc. 2002; 473-500.
- Rosenstiel SF, Land MF, Crispin MJ. Dental luting agents: A review of the current literature. J Prosthet Dent Res 1998;80: 280
- Yap A, Lee CM. Water sorption and solubility of resin-modified polyalkenoate cements. J Oral Rehabil 1997; 24: 310-4.
- International Organization for Standardization: ISO 4049
- Dentistry – Polymer-based filling, restorative and luting materials. rd ed. 2000.
- American National Standard. American Dental Association Specification n. 27 for Resin-based filling materials; 1993. 17. Bekta ÖÖ. Farkl tekniklerinin kompozit rezinlerdeki polimerizasyon büzülmesine ve dentine ba lanma dayan mlar na etkisinin incelenmesi.
- Cumhuriyet Üniv Sa l k Bilimleri Enstitüsü, Doktora tezi, 2006.
- Davis N. A nanotechnology composite. Compend Contin. Educ Dent 2003; 24: 662-70.
- Shintani H, Satou N, Yukihiro A, Satou J, Yamane I, Kouzai T, Andou T, Kai M, Hayashihara H, Inoue T. Water sorption, solubility and staining properties of microfilled resins polished by various methods. Dent Mater J 1985; 4: 54–62.
- Sideridou I, Terski V, Papanastasiou G. Study of water sorption, solubility and modulus of elasticity of light-cured dimethacrylate- based dental resins. Biomaterials 2003; 24: 655-65.
- Li Y, Swartz ML, Philips RW. Effect of filler content and size on properties of composites. J Dent Res 1985; 64: 1396-1404.
- Philips RW. Skinner’s Science of Dental Materials 8th ed. Philadelphia, 1982.
- Tamai Y, Tanaka H, Nakanishi K. Molecular simulation of permeation of small penetrant through membranes. II. Solubilities. Macromolecules 1995; 28: 2544-54.
- Arnold AM, Arnold MA, Williams VD. Measurement of water sorption by resin composite adhesives with near-infrared spectroscopy. J Dent Res 1992; 71: 438-42.
- Santos C, Clarke RL, Braden M, Guitian F, Davy KWM. Water absorption characteristics of dental composites incorporating hydroxyapatite filler. Biomaterials 2002; 23: 1897-904.
- Pallav P, De Gee AJ, Davidson CL, Erickson RL, Glasspoole EA. The influence of admixing microfiller to small-particle composite resin on wear, tensile strength, hardness, and surface roughness. J Dent Res. 1989;68:489–490.
- Ortengren U, Andersson F, Elgh U, Terselius B, Karlsson S. Influence of pH and storage time on the sorption and solubility behaviour of three composite resin materials. J Dent 2001;29: 35–
- Craig RG. Restorative Dental Materials 8th ed. St. Louis, 1989.
- Yap AUJ, Seneviratne C. Influence of light energy density on effectiveness of composite cure. Oper Dent 2001; 26: 460-466.
- Bekta ÖÖ, Eren D, Hürmüzlü F. Farkl iki kompozit rezinin su emilimi yönünden kar la t r lmas . CÜ Di Hek. Fak Derg 2006; 9: 100
- Asmussen E, Peutzfeldt A. Influence of UEDMA, BisGMA and TEGDMA on selected mechanical properties of experimental resin composites. Dent Mater. 1998;14(1):51-6.
- Braden M, Causton BE, Clarke RL. Diffusion of water in composite filling materials, J Dent Res 1976; 55: 730-732.
- Swartz ML, Moore BK. Direct Restorative Resins-A Comparative Study, J Prosthet Dent 1982; 47:163-170.
- Atai M, Nekoomanesh M, Hashemi SA. Physical and mechanical properties of an experimental dental composite based on a new monomer. Dent Mater 2004; 20: 663–668.
- Dulik D, Bernier R, Brauer GM. Effect of diluent monomer on the physical properties of bis-GMA-based composites. J Dent Res. ; 60: 983-9. Janda R, Roulet JF, Latta M. Water sorption and solubility of contemporary resin-based filling materials. J Biomed Mater Res ; 82: 545-551. Yaz4Cma Adresi: Dr. Arife KAPDAN Cumhuriyet Üniversitesi Di Hekimli i Fakültesi Pedodonti A.D. Kampus/S+VAS Tel Faks : 0346 219 1237
- E-posta : arife_sozen@yahoo.com
FARKLI YAPIDAK KOMPOZ T REZ N MATERYALLER N N SU EM L M VE SUDA ÇÖZÜNÜRLÜK DE ERLER N N KAR ILA TIRILMASI
Öz
Amaç: Kompozit rezinlerin fiziksel özelliklerinin; su absorbsiyonu ve çözünürlük testleri ile ara t r lmas amaçlanm t r. Gereç ve yöntem: Bu amaçla klinikte kullan lmakta olan universal(Venus), mikrofil hibrit (Gradia Direct Anterior), nanofil (Filtek Supreme) ve nanohibrit kompozit rezinler (Clearfil Majesty Esthetic, Premise, Artemis) olmak üzere 6 çe it kompozit kullan lm t r. Her bir gruptan standart boyutlarda 15 adet örnek haz rlanm t r. Su absorbsiyon testinde örneklerin kuru a4 rl klar Molarak belirlendi. Örnekler 168 gün boyunca 37°C’ de distile suda bekletildi ve 7’ er günlük periyotlarla a4 rl klar hassas terazide ölçüldü ve M2olarak belirlendikten sonra M2–M1/V formülüne göre sonuçlar mg/mm3olarak tespit edildi. Çözünürlük testinde örneklerin kuru a4 rl klar M1olarak belirlendi. Örnekler 168 gün boyunca 37°C’ de distile suda bekletildi ve 7’ er günlük periyotlarla a4 rl klar hassas terazide ölçüldü ve M3olarak belirlendikten sonra M3–M1/V formülüne göre sonuçlar mg/mm3olarak tespit edildi. Elde edilen verilerin istatistiksel de4erlendirilmesi yap ld .Bulgular: Yapt 4 m z in vitro çal madan elde etti4imiz sonuçlara göre nanofil ve nano hibrit kompozitlerin tüm testlerde universal ve mikrofil hibrit kompozitlere göre istatistiksel olarak anlaml fark olu turdu4u görülmü tür. Sonuç: Sonuç olarak; kompozit rezinlerin içerdi4i metakrilat grup veya gruplar n, inorganik doldurucu içeri4inin, doldurucu a4 rl 4 n n, rezin matriks ba4lant yüzeyinin fiziksel yap y etkiledi4i söylenebilir
Anahtar Kelimeler
Kaynakça
- Craig RG. Direct esthetic restorative materials. Restorative Dental Materials 2000; 244-267.
- Hickel R, Dasch W, Janda R. New direct restorative materials. Int Dent J 1998; 48: 3-16.
- Manhart J, Kunzelmann KH, Chen HY, Hickel R. Mechanical properties and wear behavior of ligth-cure packable composite resins. Dent Mater 2000; 16:33-40.
- Dayangaç GB. Kompozit rezin restorasyonlar. Güne Kitapevi, Ankara, 2000, syf. 14.
- Guggenberger R, Weinmann W. Exploring beyond methacrylates. Am J Dent 2000; 30: 10-15.
- Mitra SB, Wu D, Holmes BM. An application of nanotechnology in advanced dental materials. J Am Dent Assoc ; 134: 1382-90.
- Condon JR, Ferracane JL. Reduced polymerization stres through non-bonded nanofillerparticles. Biomaterials 2002; 23: 3807- 3815.
- Dabano lu A, Kunzelmann KH, Hickel R, Koray F. Three- body wear resistance of resin composites.DGZ/EFCD-Meeting, Munich, Duke ES. Has dentistry moved into the nanotechnology era? Compend Contin Educ Dent 2003; 24: 380-82.
- Yap AU, Yap SH, Teo CK, Ng JJ. Comparison of surface finish of new aesthetic restorative materials. Oper Dent 2004; 29: 100-4.
- Bayne SC, Heymann HO, Swift EJ Jr. Update on dental composite restorations. J Am Dent Assoc 1994; 125: 687-701.
- Roberson TM, Heymann HO, Ritter AV. Introduction to composite restorations. Art&Science of operative dentistry, Ed. 4. St. Louis, Mosby Co Inc. 2002; 473-500.
- Rosenstiel SF, Land MF, Crispin MJ. Dental luting agents: A review of the current literature. J Prosthet Dent Res 1998;80: 280
- Yap A, Lee CM. Water sorption and solubility of resin-modified polyalkenoate cements. J Oral Rehabil 1997; 24: 310-4.
- International Organization for Standardization: ISO 4049
- Dentistry – Polymer-based filling, restorative and luting materials. rd ed. 2000.
- American National Standard. American Dental Association Specification n. 27 for Resin-based filling materials; 1993. 17. Bekta ÖÖ. Farkl tekniklerinin kompozit rezinlerdeki polimerizasyon büzülmesine ve dentine ba lanma dayan mlar na etkisinin incelenmesi.
- Cumhuriyet Üniv Sa l k Bilimleri Enstitüsü, Doktora tezi, 2006.
- Davis N. A nanotechnology composite. Compend Contin. Educ Dent 2003; 24: 662-70.
- Shintani H, Satou N, Yukihiro A, Satou J, Yamane I, Kouzai T, Andou T, Kai M, Hayashihara H, Inoue T. Water sorption, solubility and staining properties of microfilled resins polished by various methods. Dent Mater J 1985; 4: 54–62.
- Sideridou I, Terski V, Papanastasiou G. Study of water sorption, solubility and modulus of elasticity of light-cured dimethacrylate- based dental resins. Biomaterials 2003; 24: 655-65.
- Li Y, Swartz ML, Philips RW. Effect of filler content and size on properties of composites. J Dent Res 1985; 64: 1396-1404.
- Philips RW. Skinner’s Science of Dental Materials 8th ed. Philadelphia, 1982.
- Tamai Y, Tanaka H, Nakanishi K. Molecular simulation of permeation of small penetrant through membranes. II. Solubilities. Macromolecules 1995; 28: 2544-54.
- Arnold AM, Arnold MA, Williams VD. Measurement of water sorption by resin composite adhesives with near-infrared spectroscopy. J Dent Res 1992; 71: 438-42.
- Santos C, Clarke RL, Braden M, Guitian F, Davy KWM. Water absorption characteristics of dental composites incorporating hydroxyapatite filler. Biomaterials 2002; 23: 1897-904.
- Pallav P, De Gee AJ, Davidson CL, Erickson RL, Glasspoole EA. The influence of admixing microfiller to small-particle composite resin on wear, tensile strength, hardness, and surface roughness. J Dent Res. 1989;68:489–490.
- Ortengren U, Andersson F, Elgh U, Terselius B, Karlsson S. Influence of pH and storage time on the sorption and solubility behaviour of three composite resin materials. J Dent 2001;29: 35–
- Craig RG. Restorative Dental Materials 8th ed. St. Louis, 1989.
- Yap AUJ, Seneviratne C. Influence of light energy density on effectiveness of composite cure. Oper Dent 2001; 26: 460-466.
- Bekta ÖÖ, Eren D, Hürmüzlü F. Farkl iki kompozit rezinin su emilimi yönünden kar la t r lmas . CÜ Di Hek. Fak Derg 2006; 9: 100
- Asmussen E, Peutzfeldt A. Influence of UEDMA, BisGMA and TEGDMA on selected mechanical properties of experimental resin composites. Dent Mater. 1998;14(1):51-6.
- Braden M, Causton BE, Clarke RL. Diffusion of water in composite filling materials, J Dent Res 1976; 55: 730-732.
- Swartz ML, Moore BK. Direct Restorative Resins-A Comparative Study, J Prosthet Dent 1982; 47:163-170.
- Atai M, Nekoomanesh M, Hashemi SA. Physical and mechanical properties of an experimental dental composite based on a new monomer. Dent Mater 2004; 20: 663–668.
- Dulik D, Bernier R, Brauer GM. Effect of diluent monomer on the physical properties of bis-GMA-based composites. J Dent Res. ; 60: 983-9. Janda R, Roulet JF, Latta M. Water sorption and solubility of contemporary resin-based filling materials. J Biomed Mater Res ; 82: 545-551. Yaz4Cma Adresi: Dr. Arife KAPDAN Cumhuriyet Üniversitesi Di Hekimli i Fakültesi Pedodonti A.D. Kampus/S+VAS Tel Faks : 0346 219 1237
- E-posta : arife_sozen@yahoo.com
Ayrıntılar
| Birincil Dil | İngilizce |
|---|---|
| Bölüm | Original Research Articles |
| Yazarlar | |
| Yayımlanma Tarihi | 1 Kasım 2011 |
| Gönderilme Tarihi | 1 Kasım 2011 |
| Yayımlandığı Sayı | Yıl 2009Cilt: 12 Sayı: 1 |
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